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In this episode, we dive into two real-world stability challenges from our lab. First, we explore a custom tune solution prepared in dilute ammonium hydroxide for ICP-MS, designed to improve lab efficiency. Learn how it performed over time and how to use it effectively for short-term use. Then, we dig into an unexpected silver instability in a low-level multi-element blend — traced back to residual chloride from chromium prep.

From method design to trace contamination troubleshooting, this episode is full of practical lessons for anyone working with custom solutions or chasing long-term stability.

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Experiencing issues in your prep or analysis? This episode is full of practical advice to keep your data on track.

Learn how to improve mercury recoveries, including best practices for stabilization in different matrices and container types. We also dive into designing high-concentration multi-element blends, highlighting unexpected incompatibilities and how acid concentration impacts stability. Finally, we discuss anion and IC standard preparation, covering pH control, contamination risks, and tips for preventing nitrite degradation and microbial growth.

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In this episode, we wrap up our glossary discussions with a focus on element speciation — why ICP alone can't distinguish oxidation states and how chromatography can help. We also break down working solutions, explaining how to properly dilute stock standards for analysis. Plus, we discuss matrix effects, covering signal suppression, ionization buffers, and why matrix matching is critical for accuracy.