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In this episode, we dive into two real-world stability challenges from our lab. First, we explore a custom tune solution prepared in dilute ammonium hydroxide for ICP-MS, designed to improve lab efficiency. Learn how it performed over time and how to use it effectively for short-term use. Then, we dig into an unexpected silver instability in a low-level multi-element blend — traced back to residual chloride from chromium prep.

From method design to trace contamination troubleshooting, this episode is full of practical lessons for anyone working with custom solutions or chasing long-term stability.

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Experiencing issues in your prep or analysis? This episode is full of practical advice to keep your data on track.

Learn how to improve mercury recoveries, including best practices for stabilization in different matrices and container types. We also dive into designing high-concentration multi-element blends, highlighting unexpected incompatibilities and how acid concentration impacts stability. Finally, we discuss anion and IC standard preparation, covering pH control, contamination risks, and tips for preventing nitrite degradation and microbial growth.

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In this episode, we wrap up our glossary discussions with a focus on element speciation — why ICP alone can't distinguish oxidation states and how chromatography can help. We also break down working solutions, explaining how to properly dilute stock standards for analysis. Plus, we discuss matrix effects, covering signal suppression, ionization buffers, and why matrix matching is critical for accuracy.

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In this episode, we continue exploring key terms in elemental analysis, focusing on calibration standards, how they establish accuracy, and why they are essential for reliable results. We also cover internal standards, their role in correcting matrix effects, and best practices for selecting them. Finally, we dive into blank corrections, breaking down calibration blanks, reagent blanks, and method blanks — critical tools for improving data accuracy.

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Fresh from Pittcon 2025, we’re recapping the biggest moments, key industry insights, and what made ICP Alley a must-visit destination! Hear about our experience connecting with customers, tackling live tech support questions, and catching up with industry partners. Plus, we dive into new trends in sample introduction, instrument developments, and technical challenges analysts are facing today.

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In this episode, we unpack fundamental concepts that every ICP analyst should know. Learn what National Metrology Institutes (NMIs) are and why SI traceability is essential for accurate measurements. We also clarify the differences between SRMs, CRMs, RMs, and PCRMs, helping you choose the right standard for your work. Plus, we discuss accuracy vs. precision, measurement uncertainty, and how tolerance impacts your data.

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In this Q&A episode, we answer common questions from ICP analysts, including how to choose between AA and CG product lines for your standards, when certification levels matter, and what documentation differences to expect. We also troubleshoot high recoveries of copper and lead in ICP-OES, exploring possible interferences, calibration curve issues, and internal standard miscalculations. Plus, we break down how internal standard baselines can throw off your results and how to fix them.

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In this Q&A episode, we answer analyst questions on EPA Method 200.8, including tuning recommendations, chloride interferences, and digestion techniques for wastewater and drinking water analysis. We also tackle antimony stability, comparing HF and tartaric acid stabilization methods, and discuss key strategies for minimizing contamination in ICP-MS. Plus, our team shares critical HF safety tips, including best practices for handling and emergency response.

Have a question you’d like answered on Bench Boost? Send it our way — we might cover it in a future episode!